Селективность хроматографических колонок

31 Июл 2019

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Обзор публикаций, в которых описывается удерживающая способность и селективность стационарных фаз для ВЭЖХ в разных хроматографических режимах: обращенно-фазовом (RP), нормально-фазовом (NP), гидрофильном (HILIC) и смешанных режимах (RP-CT, RP-IC).

Обращено-фазовая ВЭЖХ (RP HPLC)

  • Claessens H.A. Characterization of stationary phases for reversed-phase liquid chromatography: column testing, classification and chemical stability. – Eindhoven, Netherlands: Technische Universiteit Eindhoven, 1999. – 285 c. ISBN 90-386-0658-3; DOI: 10.6100/IR518234
  • Column selectivity in reversed-phase liquid chromatography I. A general quantitative relationship. N.S. Wilson et al. / J. Chromatogr. A 961 (2002) С. 171–193 DOI: 10.1016/S0021-9673(02)00659-3
  • Column selectivity in reversed-phase liquid chromatography II. Effect of a change in conditions. N.S. Wilson et al. / J. Chromatogr. A 961 (2002) С. 195–215 DOI: 10.1016/S0021-9673(02)00660-X
  • Column selectivity in reversed-phase liquid chromatography III. The physico-chemical basis of selectivity. N.S. Wilson et al. / J. Chromatogr. A 961 (2002) С. 217–236 DOI: 10.1016/S0021-9673(02)00658-1
  • Column selectivity in reversed-phase liquid chromatography IV. Type-B alkyl-silica columns. J. J. Gilroy et al. / J. Chromatogr. A 1000 (2003) С. 757–778 DOI: 10.1016/S0021-9673(03)00512-0
  • Column selectivity in reversed-phase liquid chromatography V. Higher metal content (type-A) alkyl-silica columns. N.S. Wilson et al. / J. Chromatogr. A 1026 (2004) С. 77–89 DOI: 10.1016/j.chroma.2003.11.043
  • Shape selectivity in reversed-phase liquid chromatography. K.A. Lippa, C.A. Rimmer, L.C. Sander / Adv. Chromatogr. 46 (2008) С. 235–303 DOI: 10.1201/9781420060263.ch5
  • Contributions to reversed-phase column selectivity. I. Steric interaction / Carr P.W., Dolan J.W., Neue U.D., Snyder L.R. J. Chromatogr. A. 1218 (13), 2011. C. 1724–1742. DOI: 10.1016/j.chroma.2011.01.047
  • «Orthogonal» separations for reversed-phase liquid chromatography / Pellett J., Lukulay P., Mao Y. et al. J. Chromatogr. A. 1101(1–2), 2006 C. 122–135. DOI: 10.1016/j.chroma.2005.09.080

Нормально-фазовая ВЭЖХ (NP HPLC)

  • Liquid Chromatography. Normal Phase. Reference Module in Chemistry, Molecular Sciences and Chemical Engineering / Jandera P. Encyclopedia of Analytical Science (Third Edition), 2013, С. 162–173. DOI: 10.1016/b978-0-12-409547-2.00300-0
  • Practical Aspects of Normal-Phase Chromatography / Abbot S.R. Journal of Chromatographic Science, V. 18, October 1980, C. 540–550. DOI: 10.1093/chromsci/18.10.540
  • New stationary phases for normal-phase high-performance liquid chromatography (NP-HPLC) / Deisenhofer R. L., Ballschmiter K. F. Journal of Analytical Chemistry, 360, 1998. C. 763–768. DOI: 10.1007/s002160050802
  • Optimization of normal-phase chromatographic separation of compounds with primary, secondary and tertiary amino groups / Kagan M., Chlenov M. Melnikov S. et al. Journal of Chromatography A, 1194, 2008. C. 80–89. DOI: 10.1016/j.chroma.2008.04.052

Хроматография гидрофильных взаимодействий (HILIC HPLC)

  • Wang P.G. Hydrophilic Interaction Liquid Chromatography (HILIC) and Advanced Applications / P.G., Wang W. He. – CRC Press, 2011. – 610 с. ISBN: 1439807531, 9781439807538
  • Olsen B.A. Hydrophilic Interaction Chromatography: A Guide for Practitioners / B.A. Olsen, B.W. Pack, M.F. Vitha. – New York, USA: Wiley, 2013. – 336 c. ISBN: 1118495217, 9781118495216
  • Hydrophilic interaction liquid chromatography (HILIC) – a powerful separation technique. / Buszewski B., Noga S. Analytical and Bioanalytical Chemistry, 402(1), 2011, C. 231–247. DOI: 10.1007/s00216-011-5308-5
  • Main Interactions and Influences of the Chromatographic Parameters in HILIC Separations / Greco G., Letzel T. Journal of Chromatographic Science, 51(7), 2013 C. 684–693. DOI:10.1093/chromsci/bmt015
  • Stationary and mobile phases in hydrophilic interaction chromatography: a review / Jandera P. Analytica Chimica Acta 692. 2011, C. 1–25. DOI: 10.1016/j.aca.2011.02.047
  • A Comparison of Two Separation Modes: HILIC and Aqueous Normal Phase Chromatography / Matyska M. T., Pesek J. LCGC North America. V. 25, Issue 5, C. 480–490.

Обращено-фазовая ВЭЖХ с «переносом заряда» (RP-CT HPLC)

  • Квалификация ВЭЖХ-оборудования. Тестовые испытания обращенно-фазовых колонок. К.С. Сычев, Е.А. Окунская и др. / Аналитика № 4 (2017) С. 82–87 DOI: 10.22184/2227-572X.2017.35.4.82.87
  • Column selectivity in reversed-phase liquid chromatography VIII. Phenylalkyl and fluoro-substituted columns D.H. Marchand et al. / J. Chromatogr. A 1062 (2005) 65–78 DOI: 10.1016/j.chroma.2004.11.014
  • Chromatographic classification and comparison of commercially available reversed-phase liquid chromatographic columns containing phenyl moieties using principal component analysis / M.R. Euerby, P. Petersson, W. Campbell, W. Roe / Journal of Chromatography A, 1154 (2007) 138–151. DOI: 10.1016/j.chroma.2007.03.119
  • Chromatographic classification and comparison of commercially available perfluorinated stationary phases for reversed-phase liquid chromatography using Principal Component Analysis / A.P. McKeown, P. Petersson / Journal of Separation Science 26 (2003) 295–306. DOI: 10.1002/jssc.200390035
  • Column selectivity in reversed-phase liquid chromatography VII. Cyanopropyl columns D.H. Marchand et al. / Journal of Chromatography A, 1062 (2005) 57–64 DOI: 10.1016/j.chroma.2004.11.015
  • Column selectivity in reversed-phase liquid chromatography VI. Columns with embedded or end-capping polar groups D.H. Marchand et al. / Journal of Chromatography A, 1026 (2004) 91–100 DOI: 10.1016/j.chroma.2003.11.041
  • Separation and Isomer Identification of PCDDs by Reversed-Phase Liquid Chromatography Using Electron-Donor and Electron-Acceptor Bonded Silicas. N. Tanaka, K. Kimata et al. / Organohalogen Compounds, V.19. (1994) 85–91
  • Porous Graphitic Carbon as a Stationary Phase in HPLC: Theory and Applications. L. Pereira / Journal of Liquid Chromatography & Related Technologies 31, 2008. C. 1687–1731. DOI: 10.1080/10826070802126429
  • Porous graphitic carbon: A versatile stationary phase for liquid chromatography / West C., Elfakir C., Lafosse M. Journal of Chromatography A, 1217(19), 2010. C. 3201-3216. DOI: 10.1016/j.chroma.2009.09.052

Смешанные режимы с дополнительным ионным обменом (Mixed-mode HPLC)

  • Contributions to reversed-phase column selectivity. II. Cation exchange / Marchand D.H., Carr P.W., McCalley D.V. et al. Journal of Chromatography A, 1218(40), 2011. C. 7110–7129. DOI: 10.1016/j.chroma.2011.07.085
  • Mixed-Mode HPLC Separations: What, Why, and How / Taylor T. LCGC North America. V. 32, Issue 3, C. 226
  • Mixed-Mode Chromatography – A Review / Lemasson E., Bertin S. et al. V. 30, Issue 6, C. 22–33
  • Mixed-mode chromatography in pharmaceutical and biopharmaceutical applications. Zhang K., Liu X. Journal of Pharmaceutical and Biomedical Analysis, 128, 2016. С. 73–88. DOI: 10.1016/j.jpba.2016.05.007
  • Exploring Mixed-Mode Chromatography: Column Chemistry, Properties, and Applications / Liu X., Tracy M. et al. Thermo Fisher Scientific, Sunnyvale, CA, USA.
  • Mixed-mode ion-exchangers and their comparative chromatographic characterization in reversed-phase and hydrophilic interaction chromatography elution modes / Lammerhofer M., Richter M. et al. Journal of Separation Science, 31, 2008. C. 2572–2588. DOI: 10.1002/jssc.200800178
  • Mixed-mode chromatography with zwitterionic phosphopeptidomimetic selectors from Ugi multicomponent reaction / Gargano A.F.G., Leek T. et al. Journal of Chromatography A, V.1317, 2013. C. 12–21 DOI: 10.1016/j.chroma.2013.07.095
  • HILIC behavior of a reversed-phase/cation-exchange/anion-exchange trimode column / Liu X., Pohl C.A. Journal of Separation Science, 33, 2010. C 779–786. DOI: 10.1002/jssc.200900645
  • How to separate ionic liquids: Use of Hydrophilic Interaction Liquid Chromatography and mixed mode phases / Lamouroux C, Foglia G., Le Rouzo G. Journal of Chromatography A, V.1218, Issue 20, 2011. C. 3022–3028. DOI: 10.1016/j.chroma.2011.03.053
  • Simultaneous determination of positive and negative pharmaceutical counterions using mixed-mode chromatography coupled with charged aerosol detector / Zhang K., Dai L., Chetwyn N.P. Journal of Chromatography A, V.1217, Issue 37, 2010. C. 5776–5784. DOI: 10.1016/j.chroma.2010.07.035
  • Characterization of Retention Mechanisms in Mixed-Mode HPLC with a Bimodal Reversed-Phase/Cation-Exchange Stationary Phase / Lemasson E., Richer Y. et al. Chromatographia V.81, Issue 3, 2018. C. 387–399 DOI: 10.1007/s10337-018-3477-5
  • Simultaneous determination of cations, zwitterions and neutral compounds using mixed-mode reversed-phase and cation-exchange high-performance liquid chromatography / Li J., Shao S., et al. Journal of Chromatography A, 1185(2), 2008. С. 185–193. DOI: 10.1016/j.chroma.2008.01.083

Подготовил Дмитрий Кургачев